Position: Home > Articles > Determination of Organophosphorus Residues in Cassava by GC/FID
Hubei Agricultural Sciences
2013,52
(9)
2146-2148
超声波-气相色谱法检测木薯中有机磷农药残留
作 者：
许元明;张贞发
单 位：
广西民族师范学院化学与生物工程系
关键词：
氢火焰离子化气相色谱法;甲拌磷;特丁硫磷;木薯(Manihot esculenta)
摘 要：
建立了一种快速、简单、准确的检测木薯(Manihot esculenta)中有机磷农药残留量的方法。应用超声波辅助萃取-氢火焰离子化气相色谱法(GC/FID)检测木薯中甲拌磷、特丁硫磷两种农药的残留量。甲拌磷与特丁硫磷的浓度为0.0～5.0μg/mL时的峰面积与浓度呈良好的线性关系,平均回收率为81.86%～84.32%,相对标准偏差(RSD)为4.51%～5.85%。该方法操作简便,能满足木薯中甲拌磷和特丁硫磷农药残留量的分析要求。
译 名：
Determination of Organophosphorus Residues in Cassava by GC/FID
作 者：
XU Yuan-ming,ZHANG Zhen-fa(Department of Chemical and Biological Engineering,Guangxi Normal University for Nationalities,Chongzuo 532200,Guangxi,China)
关键词：
GC / FID;phorate;terbufos;cassava(Manihot esculenta)
摘 要：
In order to establish a rapid,brief and accurate method to detect organophosphorus residues,ultrasound-assisted extraction was used in sample processing and GC / FID were used to detect phorate and terbufos in cassava.The concentration and peak area showed a good linear relationship in the concentration range of 0.0～5.0 μg / mL.Recovery of standard addition was 81.86%～84.32%,Relative standard deviations(RSD) were 4.51%～5.85%.The method was easy to operate,and satisfied the requirements of residues analysis.
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