Position: Home > Articles > Optimization of Extraction of Polysaccharides from Ziziphus Jujubes Mill “Jinsixiaozao” by Response Surface Methodology
Journal of Jilin Agricultural University
2014,36
(3)
352-359
响应面法优化金丝小枣枣渣中多糖提取工艺
作 者:
张好好;洪波;李宗亮;金东日;陈大洋;周米平
单 位:
吉林农业大学资源与环境学院
关键词:
枣渣粉;多糖;响应面法;微波提取法;超声波提取法;工艺优化
摘 要:
以金丝小枣枣渣粉为试验材料,在单因素试验的基础上,采用3因素3水平的Box-Behnken中心组合的响应面法,对微波提取法和超声波提取法提取多糖的工艺进行了优化。结果表明:微波提取多糖的最佳工艺为微波提取时间3 min,微波功率420 W,液固比(mL∶g)25∶1,提取率为3.43%;超声波提取的最佳工艺为提取时间31 min,提取温度50℃,液固比29∶1,提取率为3.37%。微波提取法比超声波提取法的多糖提取率提高了1.75%。
译 名:
Optimization of Extraction of Polysaccharides from Ziziphus Jujubes Mill “Jinsixiaozao” by Response Surface Methodology
作 者:
ZHANG Hao-hao;HONG Bo;LI Zong-liang;JIN Dong-ri;CHEN Da-yang;ZHOU Mi-ping;College of Resources and Environment,Jilin Agricultural University;
关键词:
jujube slag powder;;polysaccharide;;response surface method;;microwave extraction method;;ultrasonic wave extraction method;;process optimization
摘 要:
Using jujube slag powder of Ziziphus Jujubes Mill"Jinsixiaozao"as matrials,on the basis of single factor test,we studied the optimization of polysaccharide extraction process of microwave extraction method and ultrasonic extraction method by the response surface method designed as a three-variable and three-level Box-Behnken central composite.The optimum process of microwave extraction method was proved to be extraction time 3 minutes,microwave power 420 W and liquidsolid ratio(mL∶ g) 25∶ 1,under which the extraction rate reached 3.43%.The optimum process of ultrasonic wave extraction method was proven to be extraction time 31 minutes,temperature 50 ℃and liquid-solid ratio 29∶ 1,under which the extraction rate reached 3.37%.Extraction rate of the microwave extraction was 1.75% higher than that of the ultrasonic wave extraction.