当前位置: 首页 > 文章 > 29%吡虫啉·多菌灵·烯肟菌胺悬浮种衣剂的高效液相色谱分析 农药 2012,51 (4) 275-277
Position: Home > Articles > Analysis of Imidacloprid·Carbendazim·Fenaminstrobin 29% FSC by HPLC Agrochemicals 2012,51 (4) 275-277

29%吡虫啉·多菌灵·烯肟菌胺悬浮种衣剂的高效液相色谱分析

作  者:
丑靖宇;李超;鞠光秀;王军锋;李洋;遇璐;孙俊;单净宇;段秀洪
单  位:
沈阳化工研究院有限公司新农药创制与开发国家重点实验室;沈阳科创化学品有限公司
关键词:
吡虫啉;多菌灵;烯肟菌胺;悬浮种衣剂;高效液相色谱
摘  要:
[目的]建立吡虫啉·多菌灵.烯肟菌胺悬浮种衣剂的高效液相色谱分析方法。[方法]以甲醇-水-氨水为流动相,使用ODS-C18反相柱,在270 nm的检测波长下,对样品进行分析。[结果]吡虫啉、多菌灵和烯肟菌胺的标准偏差分别为0.04、0.07、0.03,变异系数分别为0.27%、0.70%、0.73%,平均回收率分别为99.56%、99.43%、99.79%,线性相关系数分别为0.9998、0.9999、0.9999。[结论]该方法操作简便快速,准确度和精密度高,线性关系好,是吡虫啉.多菌灵.烯肟菌胺悬浮种衣剂合适的分析方法。
译  名:
Analysis of Imidacloprid·Carbendazim·Fenaminstrobin 29% FSC by HPLC
作  者:
CHOU Jing-yu1,LI Chao1,JU Guang-xiu1,WANG Jun-feng1,LI Yang1,YU Lu1,SUN Jun1,SHAN Jing-yu1,DUAN Xiu-hong2(1.State Key Laboratory of the Discovery and Development of Novel Pesticide,Shenyang Research Institute of Chemical Industry Co.,Ltd.,Shenyang 110021,China;2.Shenyang Sciencreate Chemicals Co.,Ltd.,Shenyang 110144,China)
关键词:
imidacloprid;carbendazim;fenaminstrobin;FSC;HPLC
摘  要:
[Aims] The high performance liquid chromatography method for the simultaneous determination of imidacloprid·carbendazim·fenaminstrobin flowable concentrates for seed coating(FSC) was established.[Methods] The sample was analyzed with C18 column at 270 nm,and methanol,water,and NH3·H2O were used as the mobile phase.[Results] The results showed that the standard deviations were 0.04,0.07,and 0.03,the coefficients of variation were 0.27,0.70,and 0.73%,the recovery ratios were 99.56,99.43,and 99.79%,the linear correlations coefficients were 0.9998,0.9999,and 0.9999.[Conclusions] The described method was a suitable analysis method with fast speed,high precision and accuracy,and good linear correlations.

相似文章

计量
文章访问数: 9
HTML全文浏览量: 0
PDF下载量: 0

所属期刊

推荐期刊