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Position: Home > Articles > A Review of Synthetic Methods of Oxaziclomefone Agrochemicals 2014,53 (5) 386-387+389

噁嗪草酮合成方法述评

作  者:
裴和瑛;孙克;张敏恒
单  位:
沈阳化工研究院有限公司新农药创制与开发国家重点实验室
关键词:
噁嗪草酮;工艺路线;合成方法
摘  要:
总结了文献报道的噁嗪草酮及其中间体的合成工艺路线和具体的合成方法。噁嗪草酮是由关键中间体5-苯基-2,2,6-三甲基-2H,4H-1,3-二氧杂环己烯-4酮或者3-苯基乙酰乙酸乙酯与N-亚甲基-1-甲基-1-(3,5-二氯苯基)乙胺反应制得。主要有2条工艺路线。
译  名:
A Review of Synthetic Methods of Oxaziclomefone
作  者:
PEI He-ying;SUN Ke;ZHANG Min-heng;State Key Laboratory of the Discovery and Development of Novel Pesticide,Shenyang Research Institute of Chemical Industry Co., Ltd.;
关键词:
oxaziclomefone;;process;;synthetic method
摘  要:
The synthetic method and detailed process of oxaziclomefone and its intermediates reported in the literature were summarized. There were two main process routes to synthesize oxaziclomefone. It was prepared by the reaction of 2,2,6-trimethyl-5-phenyl-4H-1,3-dioxin-4-one or ethyl 3-oxo-2-phenylbutanoate with 2-(3,5-dichlorophenyl)-Nmethylenepropan-2-amine.

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