中国农业科学院农业信息研究所 中国农学会
Agricultural Information Institute of CAAS China Association of Agricultural Science Societies
En
Ch
中国农业科学院农业信息研究所 中国农学会 主办

AI检索

订阅

返回顶部
当前位置: 首页 > 文章 > 环境中氯氟氰虫酰胺的残留检测方法 农药 2016 (5) 366-369
Position: Home > Articles > The Method for Determination of Cyhalodiamide Residues in Environmental Samples Agrochemicals 2016 (5) 366-369

环境中氯氟氰虫酰胺的残留检测方法

作  者：
李策;蔡磊明;赵华;汤涛;宣彩迪;郭东梅
单  位：
新疆农业大学草业与环境科学学院;浙江省农业科学院农产品质量标准研究所省部共建农产品质量安全国家重点实验室培育基地农业部农药残留检测重点实验室;中国农业科学院农业质量标准与检测技术研究所
关键词：
氯氟氰虫酰胺;高效液相色谱;环境样品;检测方法
摘  要：
[目的]建立氯氟氰虫酰胺在水、土壤和沉积物中的高效液相色谱残留检测方法。[方法]样品经乙酸乙酯和乙腈萃取,弗罗里硅土和石墨化炭黑玻璃层析柱净化;Agilent-1260高效液相色谱检测。[结果]氯氟氰虫酰胺在各基质中的添加质量分数均为0.05、0.50、5.00 mg/kg,回收率为83.51%～100.62%,RSD为0.64%～7.63%;氯氟氰虫酰胺在水、土壤和沉积物中的最低检测质量分数为0.05 mg/kg。[结论]所建立方法的灵敏度、准确度和精密度均满足氯氟氰虫酰胺在水、土壤和沉积物中的残留分析要求。
译  名：
The Method for Determination of Cyhalodiamide Residues in Environmental Samples
作  者：
LI Ce;CAI Lei-ming;ZHAO Hua;TANG Tao;XUAN Cai-di;GUO Dong-mei;Faculty of Grassland and Environment Sciences,Xinjiang Agricultural University;State Key Lab Breeding Base for Quality and Safety of Agro-products;MOA Key Lab for Pesticide Residue Detection; Institute of Quality and Standard for Agro-products,Zhejiang Academy of Agricultural Sciences;Institute of Quality Standards and Testing Technology for Agro-Products,Chinese Academy of Agricultural Sciences;
关键词：
cyhalodiamide;;HPLC;;environmental sample;;determination method
摘  要：
[Aims] The residues of cyhalodiamide in environmental samples(water, soil and sediment) was determined by high performance liquid chromatography(HPLC). [Methods] The samples were extracted with organic solvent, such as acetonitrile, ethyl acetate, and cleaned up by glass chromatography column filled with Florisi and GCB, then analyzed by Agilent-1260 high performance liquid chromatography with ultraviolet detector. [Results] The results indicated that when the addition levels were 0.05, 0.50 and 5.00 mg/kg, the recoveries of cyhalodiamide in water, soil and sediment ranged from 83.51 to 100.62%, and the relative standard deviations were 0.64-7.63%. The limits of quantification for cyhalodiamide in water, soil and sediment were 0.05 mg/kg. [Conclusions] The proposed method is simple, rapid and reliable, and meets the demand for analysis of cyhalodiamide residues in water, soil and sediment.

相似文章

导出引用
计量
文章访问数: 6
HTML全文浏览量: 0
PDF下载量: 0

所属期刊

推荐期刊

友情链接Friendly link
农业信息研究所Agricultural information institute 农业智能知识服务平台Agricultural intelligent knowledge service platform 农业学术服务平台Agricultural Knowledge Service System 中国知网CNKI 维普网VIP 万方WANFANG DATA
联系我们Contact us

电话Tell：010-82109652-808

邮箱E-mail：agrijournal@caas.cn

服务Service
关于我们About us 意见建议Opinions and suggest
版权说明Copyright
单位：中国农业科学院农业信息研究所 中国农学会 © 2017中国农业科学院农业信息研究所 ICP备案号：京ICP备09089781号-46