Position: Home > Articles > Quality Standard Research for Xugujiu
Journal of Anhui Agricultural Sciences
2015
(8)
47-49
续骨酒质量标准研究
作 者：
胡翼安;张丹雁;冯小映;陈庆奇
单 位：
广州中医药大学;广州市正骨医院;南方医科大学附属佛山市妇幼保健院
关键词：
续骨酒;质量标准;地黄;栀子苷
摘 要：
[目的]建立续骨酒的定量定性检测方法,为续骨酒质量控制提供理论依据。[方法]采用薄层色谱法(TLC)对续骨酒中的栀子、地黄定性鉴别;采用高效液相色谱法(HPLC)测定栀子苷的含量。[结果]TLC鉴别分离度好、专属性强;含量测定中栀子苷在0.1511~2.5180mg范围内呈良好线性关系,线性回归方程为Y=925558X-11386,r=0.9999(n=7),平均回收率为99.4%,RSD%为1.4。[结论]该试验所建立的方法简便、准确、专属性强、精密度高、重复性好,可作为续骨酒的质量控制方法。
译 名：
Quality Standard Research for Xugujiu
作 者：
HU Yi 'an;ZHANG Dan-yan;FENG Xiao-ying;Guangzhou University of Chinese Medicine;Guangzhou Orthopedic Hospital;
关键词：
Xugujiu;;Quality standard;;Rehmanniae Radix;;Jasminoidin
摘 要：
[Objective] To establish qualitative and quantitative detection method for Xugujiu,and provide a theoretical basis for the quality control.[Method] Gardeniae Fructus and Rehmanniae Radix were identified by TLC,the content of Jasminoidin was determined by HPLC.[Result] The spots in TLC was clear,the negative control was no interference.Content determination of Jasminoidin had good linear relationship between 0.151 1 to 2.518 mg,the linear regression equation was Y = 925 558X-11 386,r = 0.999 9(n = 7),the average recovery was 99.4%,RSD 1.4%.[Conclusion] The method is simple,accurate,specified,high precision and good repeatability.It can be used for quality control of Xugujiu.
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