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Position: Home > Articles > New Synthesis Technology of Sodium tert-Butoxide Modern Agrochemicals 2004,3 (1) 11+21

叔丁醇钠合成新工艺

作  者:
唐树成;段正康
单  位:
湘潭大学化工学院
关键词:
叔丁醇;氨基钠;合成;叔丁醇钠;干燥
摘  要:
简要介绍了叔丁醇钠的性质、用途和合成方法,重点对叔丁醇与氨基钠合成叔丁醇钠新工艺进行了实验研究。实验结果表明:新工艺与老工艺(金属钠与叔丁醇反应合成叔丁醇钠)相比,在缩短反应产物干燥时间(由原来的15 h以上降低到2 h以下)、提高产品产量和质量(含量在99%以上)、安全操作等方面具有明显的工艺优势。
译  名:
New Synthesis Technology of Sodium tert-Butoxide
作  者:
Tang Shucheng Duan Zhengkang (College of Chemical Engineering, Xiangtan University, Xiangtan 411105 China)
关键词:
tert-butanol; sodium amide; synthetise; sodium tert-butoxide; drying
摘  要:
Sodium tert-butoxide抯 synthetic methods was introduced in this paper. New synthesis technology of sodium tert-butoxide with sodium amide and tert-butanol was emphatically studied. It was experimently demonstrated that new technology had clear superiority compared with former on the reducing drying time of reaction product(from 15 hours reduced to 2 hours)、improving the quality and raising output (content of sodium tert-butoxide was over 99%).

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