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Position: Home > Articles > Analysis of Trichloracetyl Chloride by HPLC Pesticide Science and Administration 2004,25 (10) 4-6

高效液相色谱法测定三氯乙酰氯的含量

作  者:
戴永军;孙绪兵;冯宝艳;朱磊;冯训娟
单  位:
山东华阳科技股份有限公司
关键词:
三氯乙酰氯;高效液相色谱
摘  要:
本文叙述了采用反相高效液相色谱法,对三氯乙酰氯进行衍生化处理后,以甲醇+水为流动相,用C18柱和紫外检测器分离测定三氯乙酰氯方法。结果表明,三氯乙酰氯的标准偏差为0.2593;变异系数为0.2640%;平均回收率为99.49%;线性相关系数为0.9997。
译  名:
Analysis of Trichloracetyl Chloride by HPLC
作  者:
Dai Yongjun,Sun Xubing,Feng Baoyan,Zhu Lei,Feng Xunjuan(Shandong Huayang Technology Co.Ltd.,Shandong Taian 271411)
关键词:
trichloracetyl chloride;HPLC
摘  要:
The quantitative analysis of trichloracetyl chloride by reverse phase HPLC was introduced.Trichloracetyl chloride was treated with PITC.using methanol and water(82∶18)as mobile phase,using C18 column and ultraviolet detector.The results showed that the standard deviation for trichloracetyl chloride was 0.259 3,the variation coefficient was 0.264 0%,the average recovery was 99.49%,liner correlation was 0.999 7.

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