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当前位置: 首页 > 文章 > MAE-SAFE/GC-MS分析酱牛肉挥发性成分 食品科学 2013,34 (14) 250-254
Position: Home > Articles > Analysis of Volatiles in Sauced Beef by Microwave-Assisted Extraction Coupled with Solvent-Assisted Flavor Evaporation and Gas Chromatography-Mass Spectrometry FOOD SCIENCE 2013,34 (14) 250-254

MAE-SAFE/GC-MS分析酱牛肉挥发性成分

作  者：
段艳;郑福平;王楠;陈海涛;黄明泉
单  位：
北京工商大学;食品添加剂与配料北京市高等学校工程研究中心;北京工商大学化学与环境工程学院
关键词：
酱牛肉;挥发性成分;微波辅助萃取耦合溶剂辅助风味蒸发;气相色谱-质谱联用仪;气相色谱-嗅觉探测仪
摘  要：
采用微波辅助萃取耦合溶剂辅助风味蒸发法提取酱牛肉挥发性成分,利用气相色谱-质谱联用仪结合保留指数定性分析酱牛肉的挥发性成分,共鉴定出65种化合物,包括11种醇,10种醛,3种酮,8种含氮、含硫或杂环化合物,9种酸,6种酯,3种醚,14种烃和1种酚。采用嗅闻频率检测法对酱牛肉挥发性成分进行GC-O分析,嗅觉检测频率≥5/11的化合物有壬醛、5-甲基糠醛、薄荷酮、茴香脑、麦芽酚、反-肉桂醛、肉桂醇。
译  名：
Analysis of Volatiles in Sauced Beef by Microwave-Assisted Extraction Coupled with Solvent-Assisted Flavor Evaporation and Gas Chromatography-Mass Spectrometry
作  者：
DUAN Yan1,ZHENG Fu-ping1,2,*,WANG Nan1,CHEN Hai-tao1,2,HUANG Ming-quan1,2,SUN Bao-guo1,2(1.Beijing Key Laboratory of Flavor Chemistry,Beijing Technology and Business University,Beijing 100048,China;2.Beijing Higher Institution Engineering Research Center of Food Additives and Ingredients,Beijing Technology and Business University,Beijing 100048,China)
关键词：
sauced beef;volatile compounds;microwave-assisted extraction coupled with solvent-assisted flavor evaporation(MAE-SAFE);gas chromatography-mass spectrometry(GC-MS);gas chromatography-olfactometry(GC-O)
摘  要：
Volatile components of sauced beef were extracted by microwave-assisted extraction coupled with solventassisted flavor evaporation(MAE-SAFE) and identified by gas chromatography-mass spectrometry(GC-MS) combined with retention indices.Totally 65 volatile compounds were identified,including 11 alcohols,10 aldehydes,3 ketones,8 nitrogenous compounds,sulfur compounds and heterocyclic compounds,9 acids,6 esters,3 ethers,14 hydrocarbons and 1 phenol.As analyzed by gas chromatography-olfactometry(GC-O),the compounds with detection frequency larger than or equal to 5/11 were nonanal,5-methyl furfural,piperiton,anethole,maltol,(E)-cinnamaldehyde and cinnamyl alcohol.

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