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Position: Home > Articles > Determination of Fluorescent Whitening Agents in Cigarette Packing Materials with UPLC Hubei Agricultural Sciences 2015,54 (2) 437-439

卷烟包装材料中荧光增白剂的UPLC测定

作  者:
叶仲力;张建平;蔡国华;吴清辉;邓其馨;方钲中;张廷贵
单  位:
福建中烟工业有限责任公司技术中心
关键词:
卷烟;包装材料;荧光增白剂;超高效液相色谱(UPLC)
摘  要:
建立了卷烟滤嘴接装纸、成型纸中荧光增白剂ABP、VBL检测的UPLC方法。样品采用N,N-二甲基甲酰胺超声提取30 min,采用ACQUITY UPLC BEH C18(50 mm×2.1 mm,1.7μm)色谱柱分离,用乙腈/水(V/V=20∶80,流速0.3 m L/min)混合液洗脱,荧光检测器检测。该法前处理简单,回收率高,精密度好,适用于卷烟滤嘴成型纸和接装纸荧光增白剂的测定。
译  名:
Determination of Fluorescent Whitening Agents in Cigarette Packing Materials with UPLC
作  者:
YE Zhong-Li;ZHANG Jian-ping;CAI Guo-hua;WU Qing-hui;DENG Qi-xin;FANG Zheng-zhong;ZHANG Ting-gui;Technical Center of China Tobacco Fujian Industrial Corporation;
关键词:
cigarette;;packing material;;fluorescent whitening agent;;UPLC
摘  要:
An UPLC method was established to determine the fluorescent whitening agents of ABP and VBL in tipping paper and plug wrapper. The samples were extracted ultrasonically with N, N-dimethylformamide for 30 min and analyzed by UPLCFLD with a column of ACQUITY UPLC BEH C18(50 mm×2.1 mm, 1.7 μm) using acetonitrile-water solution(20∶80, V / V) as mobile phase at a flow rate of 0.3 m L / min. It was simple, precise and repeatable for detecting ABP and VBL in batches of plug wrapper and tipping paper.

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