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Position: Home > Articles > SPME-GC Analysis of Aromatic Components in Red Wine by Response Surface Methodology FOOD SCIENCE 2010,31 (24) 389-394

响应曲面法优化红葡萄酒中主要芳香物质的SPME-GC分析方法

作  者:
于静;王宏镭;霍江莲;李景明;葛毅强
单  位:
北京市产品质量监督检验所;北京市食品研究所茶叶质量监督检验站;中国农业大学食品科学与营养工程学院;科技部中国农村技术开发中心农业处
关键词:
葡萄酒;芳香物质;固相微萃取;气相色谱法;香气值;响应曲面法
摘  要:
利用固相微萃取和气相色谱技术对赤霞珠干红葡萄酒中的主要香气成分进行分析,采用单因素和响应曲面法进行试验设计,以香气值为研究指标,研究SPME的萃取时间、萃取温度和电解质(NaCl)的添加量等因素对红葡萄酒中主要芳香物质的影响。结果表明:最佳分析参数是时间30.50min、温度45℃、加盐量0.29g/mL,并对结果进行验证,在此条件下,香气值之和提高了6.1。
译  名:
SPME-GC Analysis of Aromatic Components in Red Wine by Response Surface Methodology
作  者:
YU Jing1,WANG Hong-lei1,HUO Jiang-lian2,LI Jing-ming3,GE Yi-qiang4,(1. Beijing Products Quality Supervision and Inspection Institute, Beijing 100071, China; 2. Station of Tea Quality Supervision and Examination, Beijing Food Research institute, Beijing 100162, China; 3. College of Food Science and Nutritional Engineering, China Agricultural University, Beijing 100083, China; 4. China Rural Technology Development Center, Ministry of Science and Technology, Beijing 100045, China)
关键词:
red wine;aromatic components;solid phase micro-extraction(SPME);gas chromatography(GC);aroma value;response surface design
摘  要:
Major aromatic components in red wine were analyzed by solid-phase micro-extraction and gas chromatography (SPME-GC). Effects of extraction time, extraction temperature and NaCl concentration on major aromatic components in red wine were explored by single-factor and response surface experiments. Results indicated that the optimal parameters of SPME-GC analysis were extraction time of 30.50 min, extraction temperature of 45 ℃ and NaCl concentration of 0.29 g/mL. Under the optimal conditions, total aroma value was increased by 6.1 folds.

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