中国农业科学院农业信息研究所 中国农学会
Agricultural Information Institute of CAAS China Association of Agricultural Science Societies
En
Ch
中国农业科学院农业信息研究所 中国农学会 主办

AI检索

订阅

返回顶部
当前位置: 首页 > 文章 > 超高效液相色谱-串联质谱法测定枸杞中常见的5种农药残留 现代农药 2015 (1) 37-39+49
Position: Home > Articles > Determination of Five Pesticides Residues in Chinese Wolfberry by UPLC-MS/MS Modern Agrochemicals 2015 (1) 37-39+49

超高效液相色谱-串联质谱法测定枸杞中常见的5种农药残留

作  者：
林童;魏玉海;凤晓博;姚志敏;苏珊珊;张荣
单  位：
青海出入境检验检疫局
关键词：
残留;超高效液相色谱-串联质谱;枸杞;吡虫啉;甲基硫菌灵;啶虫脒;多菌灵;嘧菌酯
摘  要：
建立超高效液相色谱-串联质谱法(UPLC-MS/MS)测定枸杞中吡虫啉、甲基硫菌灵、啶虫脒、多菌灵、嘧菌酯5种农药残留量。样品经乙腈提取,C18固相萃取小柱净化,以甲醇+0.1%甲酸水溶液为流动相,采用梯度洗脱在ACQUITY UPLC BEH C18柱上分离。结果表明,在添加水平为0.001~0.1 mg/kg时,吡虫啉、甲基硫菌灵、啶虫脒、多菌灵、嘧菌酯的回收率在82.15%~102.81%之间,相对标准偏差为1.89%~5.02%,符合农药残留分析要求。
译  名：
Determination of Five Pesticides Residues in Chinese Wolfberry by UPLC-MS/MS
作  者：
LIN Tong;WEI Yu-hai;FENG Xiao-bo;YAO Zhi-min;SU Shan-shan;ZHANG Rong;Qinghai Entry-Exit Inspection and Quarantine Bureau;
关键词：
residue;;UPLC-MS/MS;;chinese wolfberry;;imidacloprid;;thiophanate-methyl;;acetamiprid;;carbendazim;;azoxystrobin
摘  要：
An UPLC-MS/MS method for determination of imidacloprid, thiophanate-methyl, acetamiprid, carbendazim, azoxystrobin in chinese wolfberry was established. The samples were extracted with acetonitrile, cleaned up by C18 solid phase extraction column, then the extracts were detected by gradient elution using methanol + methanoic acid aqueous solution as mobile phase. The results showed that at the fortified levels of 0.001-0.1 mg/kg, the average recoveries of five pesticides ranged from 82.15% to 102.81% with the relative standard deviations(RSD) of 1.89%-5.02%.

相似文章

导出引用
计量
文章访问数: 7
HTML全文浏览量: 0
PDF下载量: 0

所属期刊

推荐期刊

友情链接Friendly link
农业信息研究所Agricultural information institute 农业智能知识服务平台Agricultural intelligent knowledge service platform 农业学术服务平台Agricultural Knowledge Service System 中国知网CNKI 维普网VIP 万方WANFANG DATA
联系我们Contact us

电话Tell：010-82109652-808

邮箱E-mail：agrijournal@caas.cn

服务Service
关于我们About us 意见建议Opinions and suggest
版权说明Copyright
单位：中国农业科学院农业信息研究所 中国农学会 © 2017中国农业科学院农业信息研究所 ICP备案号：京ICP备09089781号-46