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当前位置: 首页 > 文章 > 气相色谱法测定蜂蜜和蜂王浆中氟胺氰菊酯的残留 中国蜂业 2017,68 (1) 54-57
Position: Home > Articles > The determination of Tau-fluvalinate residue in Honey and Royal jelly by Gas Chromatography Apiculture of China 2017,68 (1) 54-57

气相色谱法测定蜂蜜和蜂王浆中氟胺氰菊酯的残留

作  者：
王祥云;金银银;汪志威;张倩;王新全;闵顺根
单  位：
省部共建国家重点实验室培育基地“浙江省植物有害生物防控重点实验室”;中国农业大学理学院
关键词：
蜂蜜;蜂王浆;氟胺氰菊酯;气相色谱带电子捕获检测器
摘  要：
氟胺氰菊酯属于合成除虫菊酯,是国内蜂业生产中使用最广泛的杀螨剂,在蜂蜜和蜂王浆等蜂产品中潜在残留风险。本文建立了蜂蜜和蜂王浆中氟胺氰菊酯残留测定方法。方法以正己烷+丙酮混合溶液提取蜂蜜和蜂王浆样品中的氟胺氰菊酯残留,经弗罗里硅土固相萃取柱净化,以气相色谱—电子捕获检测器检测,外标法定量。试验结果显示,在5~100μg/kg添加水平下,方法回收率在90.6~110%,相对标准偏差低于10%,满足残留分析方法的要求;蜂蜜和蜂王浆中的方法定量限分别为5μg/kg和10μg/kg,满足国内外残留限量的要求。
译  名：
The determination of Tau-fluvalinate residue in Honey and Royal jelly by Gas Chromatography
作  者：
Wang Xiangyun;Jin Yinyin;Wang Zhiwei;Zhang Qian;Wang Xinquan;Min Shungen;College of Science, China Agricultural University;State Key Lab Breeding Base for Zhejiang Sustainable Plant Pest Control;MOA Key Lab for Pesticide Residue Detection;Institute of Quality and Standard for Agro-products, Zhejiang Academy of Agricultural Sciences;
关键词：
honey;;royal jelly;;tau-fluvalinate;;gas chromatography with electron capture detector
摘  要：
Tau-fluvalinate, an synthesized pyrethrin, was the most popular miticide in bee industry and then caused the residue risk in the honey and royal jelly. A method was developed to determine the residue of Tau╞fluvalinate in honey and royal jelly. The residue was extracted by n-hexane and acetone mixture, cleaned by a florisil column,detected by a gas chromatography with electron capture detector and calculated with external standards. At fortification levels 5~100 μg/kg, the recoveries ranged from 90.6~110% and the relative standard deviation was less than 10%. The quantitation limits of method were 5 μg/kg for honey and 10 μg/kg for royal jelly, which were sensitive enough compared to the MRLs set by governments around the world.

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